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MoS2材料具有跟石墨烯类似的层状结构,具有非常丰富的物理化学性质,目前在电催化和光催化,能源领域都有较多的应用。
这里列出一片最近的文章,主要介绍MoS2材料的CVD方法制备。
Controlled Synthesis of Highly Crystalline MoS2 Flakes by Chemical Vapor Deposition
http://pubs.acs.org/doi/abs/10.1021/ja4013485
http://pubs.acs.org/doi/abs/10.1021/ja4013485
The controlled synthesis of highly crystalline MoS2 atomic layers remains a challenge for the practical applications of this emerging material. Here, we developed an approach for synthesizing MoS2 flakes in rhomboid shape with controlled number of layers by the layer-by-layer sulfurization of MoO2 microcrystals. The obtained MoS2 flakes showed high crystallinity with crystal domain size of 10 μm, significantly larger than the grain size of MoS2 grown by other methods. As a result of the high crystallinity, the performance of back-gated field effect transistors (FETs) made on these MoS2 flakes was comparable to that of FETs based on mechanically exfoliated flakes. This simple approach opens up a new avenue for controlled synthesis of MoS2 atomic layers and will make this highly crystalline material easily accessible for fundamental aspects and various applications. |
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